Oxidation-Reduction Reactions

AP Chemistry· difficulty 3/5

A student determines the % NaOCl in a bleach by reacting 5.00 mL of bleach (density 1.05 g/mL) with excess KI in acidic solution. The liberated I2 is titrated to a starch endpoint (blue->colorless) with 0.1000 M Na2S2O3, requiring 26.45 mL. Reactions: OCl- + 2 I- + 2 H+ -> Cl- + I2 + H2O; I2 + 2 S2O3^2- -> 2 I- + S4O6^2-.

Na2S2O3 0.1000 M V=26.45 mL I2 + starch 5.00 mL bleach + KI/H+

What is the mass percent of NaOCl (M = 74.44 g/mol) in the bleach?

  • A

    1.87%

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  • B

    3.74%

  • C

    0.94%

  • D

    9.84%

Explanation

mol S2O3^2- = 0.02645 * 0.1000 = 2.645e-3. mol I2 = 1.323e-3. mol OCl- = 1.323e-3. mass NaOCl = 1.323e-3 * 74.44 = 0.0985 g. Mass bleach = 5.00*1.05 = 5.25 g. % = 0.0985/5.25 = 1.87%.

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